The practical methods of organic chemistry by Ludwig Gattermann
By Ludwig Gattermann
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Stirring continued for 15 min THF Others Et20 THF Alkyne added to refluxing mixture dropwise during 45 min. Refluxing continued for 2 h Reaction mixture heated to 50 ~ as alkyne added dropwise during 30 min. Stirring continued for 1 h "A similar preparation of prop-l-ynylmagnesium bromide has been described in Organic Syntheses . di-Grignard reagent, which precipitates. Thus, in o r d e r to obtain e t h y n y l m a g n e s i u m b r o m i d e , an excess of acetylene must be m a i n t a i n e d in the reaction mixture.
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